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Mechanics Of Materials[JOURNAL]

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The Effect of Thin Film Adhesives on Mode II Interlaminar Fracture Toughness in Carbon Fiber Composites with Shape Memory Alloy Inserts.

Quade DJ, Jana SC, Morscher GN … +2 more , Kanaan M, McCorkle L

Mech Mater · 2019 Apr · PMID 33005067 · Full text

A single sheet of nickel-titanium (NiTi) shape memory alloy (SMA) was introduced within an IM7/8552 polymer matrix composite (PMC) panel in conjunction with multiple thin film adhesives to promote the interfacial bond st... A single sheet of nickel-titanium (NiTi) shape memory alloy (SMA) was introduced within an IM7/8552 polymer matrix composite (PMC) panel in conjunction with multiple thin film adhesives to promote the interfacial bond strength between the SMA and PMC. End notched flexure (ENF) testing was performed in accordance to ASTM D7905 method for evaluation of mode II interlaminar fracture toughness (G) of unidirectional fiber-reinforced polymer matrix composites. Acoustic emissions (AE) were monitored during testing with two acoustic sensors attached to the specimens. The composite panels examined using scanning electron microscopy techniques after part failure. G values for the control composite samples were found to be higher than those of samples with embedded SMA sheets. The presence of adhesives bonded to SMA sheets further diminished the G values. AE values revealed poor bonding of the panels, with little to no signals during testing.

Indentation Analysis of Biphasic Viscoelastic Hydrogels.

Toohey KS, Kalyanam S, Palaniappan J … +1 more , Insana MF

Mech Mater · 2016 Jan · PMID 26568646 · Full text

Mechanical properties of soft biological materials are dependent on the responses of the two phases of which they are comprised: the solid matrix and interstitial fluid. Indentation techniques are commonly used to measur... Mechanical properties of soft biological materials are dependent on the responses of the two phases of which they are comprised: the solid matrix and interstitial fluid. Indentation techniques are commonly used to measure properties of such materials, but comparisons between different experimental and analytical techniques can be difficult. Most models relating load and time during spherical indentation are based on Hertzian contact theory, but the exact limitation of this theory for soft materials are unclear. Here, we examine the response of gelatin hydrogels to shear and indentation loading to quantify combined effects of the solid and fluid phases. The instantaneous behavior of the hydrogels is different for each test geometry and loading rate, but the relaxed response, measured by the relaxed modulus, is the same for all tests, within 17%. Additionally, indentation depths from 15-25% of the radius of the spherical indenter are found to minimize error in the estimate of relaxed modulus.

Accurate Prediction of Stress in Fibers with Distributed Orientations Using Generalized High-Order Structure Tensors.

Cortes DH, Elliott DM

Mech Mater · 2014 Aug · PMID 24926114 · Full text

The orientation of collagen fibers plays an important role on the mechanics of connective tissues. Connective tissues have fibers with different orientation distributions. The angular integration formulation used to mode... The orientation of collagen fibers plays an important role on the mechanics of connective tissues. Connective tissues have fibers with different orientation distributions. The angular integration formulation used to model the mechanics of fibers with distributed orientation is accurate, but computationally expensive for numerical methods such as finite elements. This study presents a formulation based on pre-integrated Generalized High-Order Structure Tensors (GHOST) which greatly improves the accuracy of the predicted stress. Simplifications of the GHOST formulation for transversely-isotropic and planar fiber distributions are also presented. Additionally, the GHOST and the angular integration formulations are compared for different loading conditions, fiber orientation functions, strain energy functions and degrees of fiber non-linearity. It was found that the GHOST formulation predicted the stress of the fibers with an error lower than 10% for uniaxial and biaxial tension. Fiber non-linearity increased the error of the GHOST formulation; however, the error was reduced to negligible values by considering higher order structure tensors. The GHOST formulation produced lower errors when used with an elliptical fiber density function and a binomial strain energy function. In conclusion, the GHOST formulation is able to accurately predict the stress of fibers with distributed orientation without requiring numerous integral calculations. Consequently, the GHOST formulation may reduce the computational effort needed to analyze the mechanics of fibrous tissues with distributed orientations.

A symmetry invariant formulation of the relationship between the elasticity tensor and the fabric tensor.

Moesen M, Cardoso L, Cowin SC

Mech Mater · 2012 Nov · PMID 23467780 · Full text

The fabric tensor is employed as a quantitative stereological measure of the structural anisotropy in the pore architecture of a porous medium. Earlier work showed that the fabric tensor can be used additionally to the p... The fabric tensor is employed as a quantitative stereological measure of the structural anisotropy in the pore architecture of a porous medium. Earlier work showed that the fabric tensor can be used additionally to the porosity to describe the anisotropy in the elastic constants of the porous medium. This contribution presents a reformulation of the relationship between fabric tensor and anisotropic elastic constants that is approximation free and symmetry-invariant. From specific data on the elastic constants and the fabric, the parameters in the reformulated relationship can be evaluated individually and efficiently using a simplified method that works independent of the material symmetry. The well-behavedness of the parameters and the accuracy of the method was analyzed using the Mori-Tanaka model for aligned ellipsoidal inclusions and using Buckminster Fuller's octet-truss lattice. Application of the method to a cancellous bone data set revealed that employing the fabric tensor allowed explaining 75-90% of the total variance. An implementation of the proposed methods was made publicly available.

Lamina Cribrosa Thickening in Early Glaucoma Predicted by a Microstructure Motivated Growth and Remodeling Approach.

Grytz R, Sigal IA, Ruberti JW … +2 more , Meschke G, Downs JC

Mech Mater · 2012 Jan · PMID 22389541 · Full text

Glaucoma is among the leading causes of blindness worldwide. The ocular disease is characterized by irreversible damage of the retinal ganglion cell axons at the level of the lamina cribrosa (LC). The LC is a porous, con... Glaucoma is among the leading causes of blindness worldwide. The ocular disease is characterized by irreversible damage of the retinal ganglion cell axons at the level of the lamina cribrosa (LC). The LC is a porous, connective tissue structure whose function is believed to provide mechanical support to the axons as they exit the eye on their path from the retina to the brain. Early experimental glaucoma studies have shown that the LC remodels into a thicker, more posterior structure which incorporates more connective tissue after intraocular pressure (IOP) elevation. The process by which this occurs is unknown. Here we present a microstructure motivated growth and remodeling (G&R) formulation to explore a potential mechanism of these structural changes. We hypothesize that the mechanical strain experienced by the collagen fibrils in the LC stimulates the G&R response at the micro-scale. The proposed G&R algorithm controls collagen fibril synthesis/degradation and adapts the residual strains between collagen fibrils and the surrounding tissue to achieve biomechanical homeostasis. The G&R algorithm was applied to a generic finite element model of the human eye subjected to normal and elevated IOP. The G&R simulation underscores the biomechanical need for a LC at normal IOP. The numerical results suggest that IOP elevation leads to LC thickening due to an increase in collagen fibril mass, which is in good agreement with experimental observations in early glaucoma monkey eyes. This is the first study to demonstrate that a biomechanically-driven G&R mechanism can lead to the LC thickening observed in early experimental glaucoma.

Human Annulus Fibrosus Dynamic Tensile Modulus Increases with Degeneration.

Sen S, Jacobs NT, Boxberger JI … +1 more , Elliott DM

Mech Mater · 2012 Jan · PMID 22247579 · Full text

The annulus fibrosus (AF) of the intervertebral disc experiences cyclic tensile loading in vivo at various states of mechanical equilibrium. Disc degeneration is associated with alterations in the biochemical composition... The annulus fibrosus (AF) of the intervertebral disc experiences cyclic tensile loading in vivo at various states of mechanical equilibrium. Disc degeneration is associated with alterations in the biochemical composition of the AF including decreased water content, decreased proteoglycan concentration, and increased collagen deposition that affect mechanical function of the AF in compression and shear. Such changes may also affect the dynamic viscoelastic properties of the AF and thus alter the disc's ability to dissipate energy under physiologic loading. The objectives of this study were to quantify the dynamic viscoelastic properties of human AF in circumferential tension and to determine the effect of degeneration on these properties. Nondegenerated and degenerated human AF tensile samples were tested in uniaxial tension over a spectrum of loading frequencies spanning 0.01Hz to 2Hz at several states of equilibrium strain to determine the dynamic viscoelastic properties (dynamic modulus, phase angle) using a linear viscoelastic model. The AF dynamic modulus increased at higher equilibrium strain levels. The AF behaved more elastically at higher frequencies with a decreased phase angle. Degeneration resulted in a higher dynamic modulus at all strain levels but had no effect on phase angle. The findings from this study elucidate the effect of degeneration on the dynamic viscoelastic properties of human AF and lend insight into the mechanical role of the AF in cyclic loading conditions.

Bi-material attachment through a compliant interfacial system at the tendon-to-bone insertion site.

Liu YX, Thomopoulos S, Birman V … +2 more , Li JS, Genin GM

Mech Mater · 2012 Jan · PMID 24285911 · Full text

The attachment of tendon to bone, one of the greatest interfacial material mismatches in nature, presents an anomaly from the perspective of interfacial engineering. Deleterious stress concentrations arising at bi-materi... The attachment of tendon to bone, one of the greatest interfacial material mismatches in nature, presents an anomaly from the perspective of interfacial engineering. Deleterious stress concentrations arising at bi-material interfaces can be reduced in engineering practice by smooth interpolation of composition, microstructure, and mechanical properties. However, following normal development, the rotator cuff tendon-to-bone "insertion site" presents an interfacial zone that is more compliant than either tendon or bone. This compliant zone is not regenerated following healing, and its absence may account for the poor outcomes observed following both natural and post-surgical healing of insertion sites such as those at the rotator cuff of the shoulder. Here, we present results of numerical simulations which provide a rationale for such a seemingly illogical yet effective interfacial system. Through numerical optimization of a mathematical model of an insertion site, we show that stress concentrations can be reduced by a biomimetic grading of material properties. Our results suggest a new approach to functional grading for minimization of stress concentrations at interfaces.

Mixture theory-based poroelasticity as a model of interstitial tissue growth.

Cowin SC, Cardoso L

Mech Mater · 2012 Jan · PMID 22184481 · Full text

This contribution presents an alternative approach to mixture theory-based poroelasticity by transferring some poroelastic concepts developed by Maurice Biot to mixture theory. These concepts are a larger RVE and the sub... This contribution presents an alternative approach to mixture theory-based poroelasticity by transferring some poroelastic concepts developed by Maurice Biot to mixture theory. These concepts are a larger RVE and the subRVE-RVE velocity average tensor, which Biot called the micro-macro velocity average tensor. This velocity average tensor is assumed here to depend upon the pore structure fabric. The formulation of mixture theory presented is directed toward the modeling of interstitial growth, that is to say changing mass and changing density of an organism. Traditional mixture theory considers constituents to be open systems, but the entire mixture is a closed system. In this development the mixture is also considered to be an open system as an alternative method of modeling growth. Growth is slow and accelerations are neglected in the applications. The velocity of a solid constituent is employed as the main reference velocity in preference to the mean velocity concept from the original formulation of mixture theory. The standard development of statements of the conservation principles and entropy inequality employed in mixture theory are modified to account for these kinematic changes and to allow for supplies of mass, momentum and energy to each constituent and to the mixture as a whole. The objective is to establish a basis for the development of constitutive equations for growth of tissues.

A Multilayered Wall Model of Arterial Growth and Remodeling.

Karšaj I, Humphrey JD

Mech Mater · 2012 Jan · PMID 22180692 · Full text

Adaptations of large arteries to sustained alterations in hemodynamics that cause changes in both caliber and stiffness are increasingly recognized as important initiators or indicators of cardiovascular risk to high flo... Adaptations of large arteries to sustained alterations in hemodynamics that cause changes in both caliber and stiffness are increasingly recognized as important initiators or indicators of cardiovascular risk to high flow, low resistance organs such as the brain, heart, and kidney. There is, therefore, a pressing need to understand better the underlying causes of geometric and material adaptations by large arteries and the associated time courses. Although such information must ultimately come from well designed experiments, mathematical models will continue to play a vital role in the design of these experiments and their interpretation. In this paper, we present a new multilayered model of the time course of basilar artery growth and remodeling in response to sustained alterations in blood pressure and flow. We show, for example, that single- and multi-layered models consistently predict similar changes in caliber and wall thickness, but multilayered models provide additional insight into other important metrics such as the residual stress related opening angle and the axial prestress, both of which are fundamental to arterial homeostasis and responses to injury or insult.

Simulated remodeling of loaded collagen networks via strain-dependent enzymatic degradation and constant-rate fiber growth.

Hadi MF, Sander EA, Ruberti JW … +1 more , Barocas VH

Mech Mater · 2012 Jan · PMID 22180691 · Full text

Recent work has demonstrated that enzymatic degradation of collagen fibers exhibits strain-dependent kinetics. Conceptualizing how the strain dependence affects remodeling of collagenous tissues is vital to our understan... Recent work has demonstrated that enzymatic degradation of collagen fibers exhibits strain-dependent kinetics. Conceptualizing how the strain dependence affects remodeling of collagenous tissues is vital to our understanding of collagen management in native and bioengineered tissues. As a first step towards this goal, the current study puts forward a multiscale model for enzymatic degradation and remodeling of collagen networks for two sample geometries we routinely use in experiments as model tissues. The multiscale model, driven by microstructural data from an enzymatic decay experiment, includes an exponential strain-dependent kinetic relation for degradation and constant growth. For a dogbone sample under uniaxial load, the model predicted that the distribution of fiber diameters would spread over the course of degradation because of variation in individual fiber load. In a cross-shaped sample, the central region, which experiences smaller, more isotropic loads, showed more decay and less spread in fiber diameter compared to the arms. There was also a slight shift in average orientation in different regions of the cruciform.

Role of structural anisotropy of biological tissues in poroelastic wave propagation.

Cardoso L, Cowin SC

Mech Mater · 2012 Jan · PMID 22162897 · Full text

Ultrasound waves have a broad range of clinical applications as a non-destructive testing approach in imaging and in the diagnoses of medical conditions. Generally, biological tissues are modeled as an homogenized equiva... Ultrasound waves have a broad range of clinical applications as a non-destructive testing approach in imaging and in the diagnoses of medical conditions. Generally, biological tissues are modeled as an homogenized equivalent medium with an apparent density through which a single wave propagates. Only the first wave arriving at the ultrasound probe is used for the measurement of the speed of sound. However, the existence of a second wave in tissues such as cancellous bone has been reported and its existence is an unequivocal signature of Biot type poroelastic media. To account for the fact that ultrasound is sensitive to microarchitecture as well as density, a fabric-dependent anisotropic poroelastic ultrasound (PEU) propagation theory was recently developed. Key to this development was the inclusion of the fabric tensor - a quantitative stereological measure of the degree of structural anisotropy of bone - into the linear poroelasticity theory. In the present study, this framework is extended to the propagation of waves in several soft and hard tissues. It was found that collagen fibers in soft tissues and the mineralized matrix in hard tissues are responsible for the anisotropy of the solid tissue constituent through the fabric tensor in the model.

Effective Spring Stiffness for a Planar Periodic Array of Collinear Cracks at an Interface between Two Dissimilar Isotropic Materials.

Lekesiz H, Katsube N, Rokhlin SI … +1 more , Seghi RR

Mech Mater · 2011 Feb · PMID 23710104 · Full text

Explicit analytical expressions are obtained for the longitudinal and transverse effective spring stiffnesses of a planar periodic array of collinear cracks at the interface between two dissimilar isotropic materials; th... Explicit analytical expressions are obtained for the longitudinal and transverse effective spring stiffnesses of a planar periodic array of collinear cracks at the interface between two dissimilar isotropic materials; they are shown to be identical in a general case of elastic dissimilarity (the well-known open interface crack model is employed for the solution). Since the interfacial spring stiffness can be experimentally determined from ultrasound reflection and transmission analysis, the proposed expressions can be useful in estimating the percentage of disbond area between two dissimilar materials, which is directly related to the residual strength of the interface. The effects of elastic dissimilarity, crack density and crack interaction on the effective spring stiffness are clearly represented in the solution. It is shown that in general the crack interaction weakly depends on material dissimilarity and, for most practical cases, the crack interaction is nearly the same as that for crack arrays between identical solids. This allows approximate factorization of the effective spring stiffness for an array of cracks between dissimilar materials in terms of an elastic dissimilarity factor and two factors obtained for cracks in a homogeneous material: the effective spring stiffness for non-interacting (independent) cracks and the crack interaction factor. In order to avoid the effect of the crack surface interpenetration zones on the effective spring stiffness, the range of the tensile to transverse load ratios is obtained under the assumption of small-scale contact conditions. Since real cracks are often slightly open (due to prior loading history and plastic deformation), it is demonstrated that for ultrasound applications the results obtained are valid for most practical cases of small interfacial cracks as long as the mid-crack opening normalized by the crack length is at least in the order of 10.

On the six-dimensional orthogonal tensor representation of the rotation in three dimensions: A simplified approach.

Koay CG

Mech Mater · 2009 Aug · PMID 20161108 · Full text

The six-dimensional orthogonal tensor representation of the rotation about an axis in three dimensions was first proposed by (Mehrabadi et al. 1995). In this brief note, a simple and coherent approach is presented to con... The six-dimensional orthogonal tensor representation of the rotation about an axis in three dimensions was first proposed by (Mehrabadi et al. 1995). In this brief note, a simple and coherent approach is presented to construct the six-dimensional orthogonal tensor representation of the rotation of any parametrization in three dimensions and to prove its orthogonality.

WEAR BEHAVIOR OF CARBON NANOTUBE/HIGH DENSITY POLYETHYLENE COMPOSITES.

Johnson BB, Santare MH, Novotny JE … +1 more , Advani SG

Mech Mater · 2009 Oct · PMID 20161101 · Full text

Carbon Nanotube/High Density Polyethylene (CNT/HDPE) composites were manufactured and tested to determine their wear behavior. The nanocomposites were made from untreated multi-walled carbon nanotubes and HDPE pellets. T... Carbon Nanotube/High Density Polyethylene (CNT/HDPE) composites were manufactured and tested to determine their wear behavior. The nanocomposites were made from untreated multi-walled carbon nanotubes and HDPE pellets. Thin films of the precursor materials were created with varying weight percentages of nanotubes (1%, 3%, and 5%), through a process of mixing and extruding. The precursor composites were then molded and machined to create test specimens for mechanical and wear tests. These included small punch testing to compare stiffness, maximum load and work-to-failure and block-on-ring testing to determine wear behavior. Each of the tests was conducted for the different weight percentages of composite as well as pure HDPE as the baseline. The measured mechanical properties and wear resistance of the composite materials increased with increasing nanotube content in the range studied.

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